A. Technique Discussions

• Heating Under Reflux
• Setting Up & Performing a Fractional Distillation
• Recrystallization
• Sublimation
• Taking the Melting Point of a Substance
• Drying Organic Solvents
• Extraction
• Boiling Points and Distillations
• Chromatography

    235-1     Preparation of Acetylsalicylic Acid (Aspirin)
                  (Requires Choosing & Using a Recrystallization Solvent)

    235-2     Isolation of Caffein

    235-3     Isolation of Cholesterol from Gallstones

    235-4     Fractional Distillation

    235-5     Hydrolysis of an Alkyl Halide

    235-6     TLC of Analgesic Drugs

    235-7     Melting Points

    235-8     Competing Nucleophiles

    235-9     Friedel-Crafts Acylation
 
 
 

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